(2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

Base Information

Chemical Name:(2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate
CAS No.:1412190-59-0
Molecular Formula:C₂₈H₃₈N₂O₈
Molecular Weight:530.618
Hs Code.:

(2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

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Chemical Property of (2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

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Technology Process of (2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

There total 1 articles about (2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 75-91-2
tert.-butylhydroperoxide

: 69261-43-4
t-butyloxycarbonyl-tyrosinyl-phenylalanine methyl ester

: 1412190-50-1
(2S,3aR,7aR)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

: 1412190-59-0
(2S,3aS,7aS)-tert-butyl 3a-(tert-butylperoxy)-2-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-6-oxo-2,3,3a,6,7,7a-hexahydro-1H-indole-1-carboxylate

Guidance literature:: tert.-butylhydroperoxide; t-butyloxycarbonyl-tyrosinyl-phenylalanine methyl ester; With dirhodium caprolactamate; In 1,2-dichloro-ethane; at 40 ℃; for 1.5h;

With toluene-4-sulfonic acid; sodium sulfate; In 1,2-dichloro-ethane; at 20 ℃; for 16h; Overall yield = 39 %;
DOI:10.1021/jo302002j