Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-

Base Information

Chemical Name:Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-
CAS No.:136794-77-9
Molecular Formula:C29H26 N2 O7
Molecular Weight:514.535
Hs Code.:

Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-

Synonyms:Benzonitrile,3-[[[5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-,[5S-(5a,5ab,8aa,9b)]-;Furo[3',4':6,7]naphtho[2,3-d]-1,3-dioxole, benzonitrile deriv.

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Chemical Property of Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]-

There total 4 articles about Benzonitrile,3-[[[(5S,5aS,8aR,9R)-5,5a,6,8,8a,9-hexahydro-9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxofuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-5-yl]amino]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6559-91-7
4'-demethylepipodophyllotoxin

: 136794-77-9
4'-O-demethyl-4β-[(3''-cyanobenzyl)amino]-4-desoxypodophyllotoxin

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / NaN₃, CF₃COOH / CHCl₃ / 0.25 h

2: 70 percent / H₂ / 10percent Pd/C / ethyl acetate

3: BaCO₃ / CH₂Cl₂ / 40 h / 75 - 80 °C

With sodium azide; hydrogen; barium carbonate; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jm00116a001

Reference yield:

: 117604-05-4
4β-azido-4-deoxy-4′-demethylepipodophyllotoxin

: 136794-77-9
4'-O-demethyl-4β-[(3''-cyanobenzyl)amino]-4-desoxypodophyllotoxin

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂ / 10percent Pd/C / ethyl acetate

2: BaCO₃ / CH₂Cl₂ / 40 h / 75 - 80 °C

With hydrogen; barium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00116a001