C₂₄H₂₆ClNO₄S

Base Information

• Chemical Name: C₂₄H₂₆ClNO₄S
• CAS No.: 1308685-32-6
• Molecular Formula: C₂₄H₂₆ClNO₄S
• Molecular Weight: 459.994
• Mol file: 1308685-32-6.mol

Synonyms:

Chemical Property of C₂₄H₂₆ClNO₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₆ClNO₄S

There total 7 articles about C₂₄H₂₆ClNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-N-prop-2-ynylbenzenesulfonamide (55022-46-3) → C24H26ClNO4S (1308685-32-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 25 °C

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 25 °C

3.1: dmap; triethylamine / Neat (no solvent)

With dmap; n-butyllithium; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1.1: Mitsunobu reaction;

DOI:10.1002/ejoc.201100129

Reference yield:

(E)-3-(p-chlorophenyl)prop-2-en-1-ol (24583-70-8) → C24H26ClNO4S (1308685-32-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 25 °C

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 25 °C

3.1: dmap; triethylamine / Neat (no solvent)

With dmap; n-butyllithium; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1.1: Mitsunobu reaction;

DOI:10.1002/ejoc.201100129

Reference yield:

N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide (18303-04-3) → C24H26ClNO4S (1308685-32-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 6 h / 0 - 25 °C

2.1: trifluoroacetic acid / dichloromethane / 2 h / 25 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 25 °C

4.1: n-butyllithium / tetrahydrofuran / -78 °C

4.2: -78 - 25 °C

5.1: dmap; triethylamine / Neat (no solvent)

With dmap; n-butyllithium; di-isopropyl azodicarboxylate; sodium hydride; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 3.1: Mitsunobu reaction;

DOI:10.1002/ejoc.201100129

upstream raw materials:

acetic anhydride

4-methyl-N-prop-2-ynylbenzenesulfonamide

N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

(E)-3-(p-chlorophenyl)prop-2-en-1-ol