Technology Process of C22H39O3PS
There total 6 articles about C22H39O3PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
O,O-bis(2-cyanoethyl)-O-4-pentadecylbenzyl phosphorthionate;
With
methanol; potassium hydroxide;
at 20 ℃;
for 3h;
With
hydrogenchloride;
In
water;
at 20 ℃;
for 3h;
DOI:10.1002/cmdc.201000425
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 20 % Pd(OH)2/C; hydrogen / methanol / 2 h / 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
3.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.2: 2 h / Reflux; Inert atmosphere
4.1: methanol; potassium hydroxide / 3 h / 20 °C
4.2: 3 h / 20 °C
With
1H-tetrazole; methanol; lithium aluminium tetrahydride; 20 % Pd(OH)2/C; hydrogen; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/cmdc.201000425
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: palladium diacetate; triethylamine / N,N-dimethyl-formamide / 16 h / Reflux; Inert atmosphere
2.1: 20 % Pd(OH)2/C; hydrogen / methanol / 2 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
4.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere
4.2: 2 h / Reflux; Inert atmosphere
5.1: methanol; potassium hydroxide / 3 h / 20 °C
5.2: 3 h / 20 °C
With
1H-tetrazole; methanol; lithium aluminium tetrahydride; 20 % Pd(OH)2/C; hydrogen; palladium diacetate; triethylamine; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
1.1: Heck reaction;
DOI:10.1002/cmdc.201000425