N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

Base Information

Chemical Name:N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide
CAS No.:122167-12-8
Molecular Formula:C₁₆H₁₉N₂OPSn
Molecular Weight:405.023
Hs Code.:

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Chemical Property of N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

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Technology Process of N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

There total 4 articles about N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1066-45-1
trimethyltin(IV)chloride

: sodium diphenyl-cyanamidooxophosphinate

: 122167-10-6,122167-12-8
diphenyl-cyanimidophosphinoyl-O-trimethylstannylester

: 122167-12-8,122167-10-6
N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

Guidance literature:: In water; an aq. soln. of (CH3)3SnCl was dropped to a aq. soln. of Na(Ph2P(O)NCN) at room temp.; colorless ppt. filtered off, dried in vacuum; elemental analysis;

Reference yield: 85.0%

: 1066-45-1
trimethyltin(IV)chloride

: sodium diphenyl-cyanamidooxophosphinate

: 122167-10-6,122167-12-8
diphenyl-cyanimidophosphinoyl-O-trimethylstannylester

: 122167-12-8,122167-10-6
N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

Guidance literature:: In water; an aq. soln. of (CH3)3SnCl was dropped to a aq. soln. of Na(Ph2P(O)NCN) at room temp.; colorless ppt. filtered off, dried in vacuum; elemental analysis;

Reference yield: 50.0%

: 20706-08-5
bis(trimethylstannyl)carbodiimide

: 1499-21-4
Diphenylphosphinic chloride

: 122167-12-8,122167-10-6
N-diphenylphosphinoyl-N'-trimethylstannyl-carbodiimide

Guidance literature:: In tetrahydrofuran; byproducts: Me3SnCl; a soln. of Ph2P(O)Cl in THF was dropped to a soln. of (CH3)3SnNCNSn(CH3)3 in THF at 0 °, warmed to room temp., stirred for 1 h; filtration; vol. of the solvent reduced; recrystn. from toluene; elemental analysis;