3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ⁴-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester

Base Information

• Chemical Name: 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ⁴-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester
• CAS No.: 62616-06-2
• Molecular Formula: C₃₅H₂₉NO₆S
• Molecular Weight: 591.684

Synonyms:

Chemical Property of 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ⁴-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester

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Technology Process of 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ⁴-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester

There total 3 articles about 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ⁴-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester (62616-01-7) → 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ4-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester (62616-06-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Ambient temperature;

Reference yield:

dimethyl tricyclo[4.2.2.02,5]deca-3,7,9-triene-7,8-dicarboxylate (25157-95-3) → 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ4-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester (62616-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Heating

2: MCPBA / CH₂Cl₂ / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

Reference yield:

2,3,5-triphenyl-4-thiazolone (18100-80-6) → 3,9syn-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-9λ4-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester (62616-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Heating

2: MCPBA / CH₂Cl₂ / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

upstream raw materials:

3-oxo-1,2,4-triphenyl-(4at,4bc,8ac,8bt)-1,2,3,4,4a,4b,5,8,8a,8b-decahydro-1r,4c-episulfano-5t,8t-etheno-benzo[3,4]cyclobuta[1,2-c]pyridine-6,7-dicarboxylic acid dimethyl ester

dimethyl tricyclo[4.2.2.0^2,5]deca-3,7,9-triene-7,8-dicarboxylate

2,3,5-triphenyl-4-thiazolone

Downstream raw materials:

9anti-oxo-1,6,7-triphenyl-(1rS,2tH,5tH,6cS)-9λ⁴-thia-7-aza-tricyclo[4.2.1.0^2,5]non-3-en-8-one

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