benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate

Base Information

• Chemical Name: benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate
• CAS No.: 108967-21-1
• Molecular Formula: C₂₀H₂₀O₅S₂
• Molecular Weight: 404.508
• Mol file: 108967-21-1.mol

Synonyms:

Chemical Property of benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate

There total 2 articles about benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

chlorhydrate du (benzoyloxy-5 β-D-ribofuranosyl) thioformimidate de benzyle (55628-57-4,55650-11-8,73068-55-0,80581-14-2) → benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate (108967-21-1)

Guidance literature:

With hydrogen sulfide;

DOI:10.1016/S0008-6215(00)90269-6

Reference yield:

5-O-benzoyl-β-D-ribofuranosyl cyanide (30002-87-0) → benzyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate (108967-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / HCl gas / diethyl ether / 0 °C

2: 93 percent / H₂S

With hydrogenchloride; hydrogen sulfide; In diethyl ether;

DOI:10.1016/S0008-6215(00)90269-6

upstream raw materials:

chlorhydrate du (benzoyloxy-5 β-D-ribofuranosyl) thioformimidate de benzyle

5-O-benzoyl-β-D-ribofuranosyl cyanide