1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane

Base Information

• Chemical Name: 1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane
• CAS No.: 1022224-54-9
• Molecular Formula: C₂₃H₂₃FeNO₂
• Molecular Weight: 401.288
• Mol file: 1022224-54-9.mol

Synonyms:

Chemical Property of 1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane

There total 1 articles about 1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1,1'-diacetylferrocene (1273-94-5) + 4-dimethylamino-benzaldehyde (100-10-7) → 1,5-dioxo-3-(p-dimethylaminophenyl)[5]ferrocenophane (1022224-54-9)

Guidance literature:

With sodium hydroxide; In ethanol; water; other Radiation; addn. of NaOH (20.0 mmol) and p-NMe2-PhCOH (2 mmol) to soln. of 1,1'-diacetylferrocene in EtOH/H2O (4:1 v/v); heating at 80°C using 50 W microwave power for 30 min; diluting with satd. NH4Cl4; extn. with CH2Cl2; washing of org. layer with brine, drying over Na2SO4; suspending in n-hexane:EtOAc 1:1; filtration, discarding of solution, dissolving in CH2Cl2; drying; washing with n-hexane:EtOAc 1:1;

DOI:10.1016/j.jorganchem.2008.01.038

upstream raw materials:

1,1'-diacetylferrocene

4-dimethylamino-benzaldehyde