2-diphenylphosphino-1-cyanocyclopentane

Base Information

Chemical Name:2-diphenylphosphino-1-cyanocyclopentane
CAS No.:130648-96-3
Molecular Formula:C₁₈H₁₈NP
Molecular Weight:279.321
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-diphenylphosphino-1-cyanocyclopentane

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Technology Process of 2-diphenylphosphino-1-cyanocyclopentane

There total 1 articles about 2-diphenylphosphino-1-cyanocyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 3047-38-9
cyclopent-1-enecarbonitrile

: 829-85-6
diphenylphosphane

: 130648-81-6,130648-96-3
2-diphenylphosphino-1-cyanocyclopentane

Guidance literature:: In acetonitrile; at 60 ℃; Product distribution; other olefins; other diphenylphosphine derivatives;
DOI:10.1016/0022-328X(90)87207-T

Reference yield:

: 130648-96-3
cis-2-diphenylphosphino-1-cyanocyclopentane

: palladium dichloride

: trans-dichloropalladium(cis-2-diphenylphosphino-1-cyanocylopentane)2

Guidance literature:: In hydrogenchloride; ethanol; PdCl2 is dissolved in warm aq. HCl, addn. of EtOH, filtn., dropwise addn. of soln. of ligand in EtOH to the filtrate, stirring for 4 h; addn. of H2O for precipitation, filtn., washing with ether, crystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1016/0022-328X(94)87068-3