5-hydroxy-2-phenoxidothiolanium zwitterion

Base Information

• Chemical Name: 5-hydroxy-2-phenoxidothiolanium zwitterion
• CAS No.: 123192-57-4
• Molecular Formula: C₁₀H₁₂O₂S
• Molecular Weight: 196.27

Synonyms:

Chemical Property of 5-hydroxy-2-phenoxidothiolanium zwitterion

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 5-hydroxy-2-phenoxidothiolanium zwitterion

There total 1 articles about 5-hydroxy-2-phenoxidothiolanium zwitterion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1-(2,5-dihydroxyphenyl)thiolanium chloride monohydrate (28335-08-2) → 5-hydroxy-2-phenoxidothiolanium zwitterion (123192-57-4)

Guidance literature:

With ARA-2p anion exchange resin (OH form); In methanol;

DOI:10.1007/BF00633513

Reference yield: 54.0%

piperidine hydrochloride (6091-44-7) + 5-hydroxy-2-phenoxidothiolanium zwitterion (123192-57-4) → 2,5-dihydroxyphenyl 4-N-piperidinobutyl sulfide hydrochloride (123192-53-0)

Guidance literature:

1.) methanol, 2.) ethanol, 4 h, reflux;

DOI:10.1007/BF00633513

Reference yield: 40.0%

morpholin hydrochloride (10024-89-2) + 5-hydroxy-2-phenoxidothiolanium zwitterion (123192-57-4) → 2,5-dihydroxyphenyl 4-N-morpholinobutyl sulfide hydrochloride (123192-54-1)

Guidance literature:

1.) methanol, 2.) ethanol, 4.5 h, reflux;

DOI:10.1007/BF00633513

upstream raw materials:

1-(2,5-dihydroxyphenyl)thiolanium chloride monohydrate

Downstream raw materials:

2,5-dihydroxyphenyl 4-N-morpholinobutyl sulfide hydrochloride

2,5-dihydroxyphenyl 4-N-piperidinobutyl sulfide hydrochloride

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