Technology Process of C32H30N2O5
There total 8 articles about C32H30N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / methanol / 20 °C
2: 1,1'-carbonyldiimidazole / chloroform / 20 °C
3: hydrogenchloride / water; ethyl acetate / 20 °C
4: pyridine / 20 °C
5: palladium 10% on activated carbon; ammonium formate / methanol / Reflux
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; ammonium formate; potassium carbonate; 1,1'-carbonyldiimidazole;
In
methanol; chloroform; water; ethyl acetate;
DOI:10.1016/j.bmcl.2012.01.101
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
methanol;
Reflux;
DOI:10.1016/j.bmcl.2012.01.101
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium tetrahydroborate; sulfuric acid; iodine / tetrahydrofuran / Reflux
2: potassium carbonate / methanol / 20 °C
3: 1,1'-carbonyldiimidazole / chloroform / 20 °C
4: hydrogenchloride / water; ethyl acetate / 20 °C
5: pyridine / 20 °C
6: palladium 10% on activated carbon; ammonium formate / methanol / Reflux
With
pyridine; hydrogenchloride; sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; iodine; ammonium formate; potassium carbonate; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; methanol; chloroform; water; ethyl acetate;
DOI:10.1016/j.bmcl.2012.01.101