Stannane, tributyl-1H-inden-1-yl-

Base Information

• Chemical Name: Stannane, tributyl-1H-inden-1-yl-
• CAS No.: 102456-48-4
• Molecular Formula: C21H34Sn
• DSSTox Substance ID: DTXSID30452376
• Mol file: 102456-48-4.mol

Synonyms:Stannane, tributyl-1H-inden-1-yl-;102456-48-4;DTXSID30452376

Chemical Property of Stannane, tributyl-1H-inden-1-yl-

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 10
• Exact Mass: 406.168254
• Heavy Atom Count: 22
• Complexity: 311

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Sn](CCCC)(CCCC)C1C=CC2=CC=CC=C12

Technology Process of Stannane, tributyl-1H-inden-1-yl-

There total 1 articles about Stannane, tributyl-1H-inden-1-yl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tributyltin chloride (1461-22-9) + 1-indene (95-13-6) → 1(tri-n-butylstannyl)indene (102456-48-4)

Guidance literature:

With Na; In ammonia; NH3 (liquid); at 125-130°C, 6h;;

Reference yield: 26.0%

2,2'-dibromobiphenyl (13029-09-9) + 1(tri-n-butylstannyl)indene (102456-48-4) → 13H-indeno[1,2-l]phenanthrene (201-65-0) + (8bR,13S,13aR)-(R)-13-(1H-Inden-1-yl)-13,13a-dihydro-8bH-indeno[1,2-l]phenanthrene

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride;

DOI:10.1016/S0040-4039(00)73633-1

Reference yield: 4.0%

1(tri-n-butylstannyl)indene (102456-48-4) + 2,2'-diiodobiphenyl (2236-52-4) → 13H-indeno[1,2-l]phenanthrene (201-65-0) + (8bR,13S,13aR)-(R)-13-(1H-Inden-1-yl)-13,13a-dihydro-8bH-indeno[1,2-l]phenanthrene

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride;

DOI:10.1016/S0040-4039(00)73633-1

upstream raw materials:

tributyltin chloride

1-indene

Downstream raw materials:

13H-indeno[1,2-l]phenanthrene

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