Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

Base Information

Chemical Name:Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)
CAS No.:607719-92-6
Molecular Formula:C₃₀H₃₅Cl₃N₂OPRe
Molecular Weight:763.16
Hs Code.:

Re(OP(C<sub>6</sub>H<sub>5</sub>)3)Cl<sub>3</sub>(NCHCHN(C<sub>5</sub>H<sub>9</sub>)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

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Technology Process of Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

There total 2 articles about Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: ReOCl₃(NCHCHN(C₅H₉)2)

: 603-35-0
triphenylphosphine

: 607719-92-6
Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

Guidance literature:: In benzene; PPh3 was added to soln. of Re-complex in benzene, stirred for 20 min at room temp.; solvent was removed under reduced pressure, washed with hexane, dissolved in CH2Cl2, silica gel column chromy. with benzene, eluted with benzene-MeCN, solvent was removed under reduced pressure; elem. anal.;
DOI:10.1021/ic034586c

Reference yield: 70.0%

: [ReOCl₃(PPh₃)₂]

: 67430-51-7
NCHCHN(C₅H₉)2

: 607719-92-6
Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

Guidance literature:: In benzene; ligand was added to soln. of Re-complex in benzene, stirred for 30 min at room temp.; solvent was removed under reduced pressure, washed with hexane, dissolved in CH2Cl2, silica gel column chromy. with benzene, eluted with benzene-MeCN, solvent was removed under reduced pressure;
DOI:10.1021/ic034586c

Reference yield: 70.0%

: 607719-92-6
Re(OP(C₆H₅)3)Cl₃(NCHCHN(C₅H₉)2)

: 7722-84-1
dihydrogen peroxide

: 607720-20-7
Re(OP(C₆H₅)3)Cl₃(NCOCHN(C₅H₉)2)

Guidance literature:: In acetonitrile; Re-complex was dissolved in MeCN, H2O2 was added, stirred for 2 h at room temp.; solvent was evapd. under reduced pressure, washed with water, dried in vacuo over P4O10, recrystd. from CH2Cl2; elem. anal.;
DOI:10.1021/ic034586c