methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

Base Information

Chemical Name:methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside
CAS No.:54621-57-7
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:

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Chemical Property of methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

Chemical Property:

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Technology Process of methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

There total 4 articles about methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4148-70-3
methyl (exo-Ph)-3,4-O-benzylidene-β-L-arabinopyranoside

: 74-88-4
methyl iodide

: 54621-57-7,80877-11-8,80877-12-9
methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

Guidance literature:: With silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80811-3

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 54621-57-7,80877-11-8,80877-12-9
methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / toluene-p-sulphonic acid / dimethylformamide / 0.67 h / 80 °C

2: 95 percent / silver oxide / dimethylformamide

With toluene-4-sulfonic acid; silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80811-3

Reference yield:

: 80851-23-6,80851-24-7
methyl 2-O-acetyl-endo-3,4-O-benzylidene-β-L-arabinopyranoside

: 54621-57-7,80877-11-8,80877-12-9
methyl endo-3,4-O-benzylidene-2-O-methyl-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90.5 percent

2: 95 percent / silver oxide / dimethylformamide

With silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80811-3