C₂₂H₂₅Br₂N₂⁽¹⁺⁾*I^(1-)

Base Information

• Chemical Name: C₂₂H₂₅Br₂N₂⁽¹⁺⁾*I^(1-)
• CAS No.: 1280726-86-4
• Molecular Formula: C₂₂H₂₅Br₂N₂*I
• Molecular Weight: 604.166
• Mol file: 1280726-86-4.mol

Synonyms:

Chemical Property of C₂₂H₂₅Br₂N₂⁽¹⁺⁾*I^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂₂H₂₅Br₂N₂⁽¹⁺⁾*I^(1-)

There total 2 articles about C₂₂H₂₅Br₂N₂⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C21H22Br2N2 (1280726-85-3) + methyl iodide (74-88-4) → C22H25Br2N2(1+)*I(1-) (1280726-86-4)

Guidance literature:

at 60 ℃; for 6h; Inert atmosphere;

DOI:10.1021/ja200602e

Reference yield:

4,4'-dibromobenzil (35578-47-3) → C22H25Br2N2(1+)*I(1-) (1280726-86-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 5 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 1 h / 80 °C / Inert atmosphere

2.2: 12 h / 80 °C / Inert atmosphere

3.1: 6 h / 60 °C / Inert atmosphere

With ammonium acetate; sodium hydride; acetic acid; In tetrahydrofuran;

DOI:10.1021/ja200602e

upstream raw materials:

C₂₁H₂₂Br₂N₂

methyl iodide

4,4'-dibromobenzil