Pd(C₅H₄(CH₃)2BC₆H₅)2

Base Information

Chemical Name:Pd(C₅H₄(CH₃)2BC₆H₅)2
CAS No.:74989-66-5
Molecular Formula:C₂₆H₃₀B₂Pd
Molecular Weight:470.566
Hs Code.:

Pd(C<sub>5</sub>H<sub>4</sub>(CH<sub>3</sub>)2BC<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of Pd(C₅H₄(CH₃)2BC₆H₅)2

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Technology Process of Pd(C₅H₄(CH₃)2BC₆H₅)2

There total 1 articles about Pd(C₅H₄(CH₃)2BC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 1277-43-6,78206-33-4
cobaltocene

: 62496-51-9
4,4-dimethyl-1-phenyl-1,4-dihydro-borinine

: 74989-66-5
Pd(C₅H₄(CH₃)2BC₆H₅)2

Guidance literature:: With C₈H₁₂; In dichloromethane; (N2); to suspn. of Pd complex in COD was added boranederiv., then dropwise soln. of Co complex at -50°C within 1 h, mixt. was warmed up to room temp. within 2 h, CH2Cl2 was removed in vac., toluene added and soln. heated at 50°C for 4 h; soln. was filtered through Al2O3 at -78°C, solvent was removed and residue recrystd. from pentane; elem. anal.;
DOI:10.1016/S0022-328X(00)88552-6