C₂₇H₄₂O₅Si

Base Information

Chemical Name:C₂₇H₄₂O₅Si
CAS No.:1446490-23-8
Molecular Formula:C₂₇H₄₂O₅Si
Molecular Weight:474.713
Hs Code.:

C<sub>27</sub>H<sub>42</sub>O<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₄₂O₅Si

Chemical Property:

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Technology Process of C₂₇H₄₂O₅Si

There total 7 articles about C₂₇H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 201230-82-2
carbon monoxide

: 1446490-21-6
C₂₂H₂₉F₃O₆S

: 1446490-23-8
C₂₇H₄₂O₅Si

Guidance literature:: With palladium(II) trifluoroacetate; N-ethyl-N,N-diisopropylamine; bis[2-(diphenylphosphino)phenyl] ether; In acetonitrile; for 14h;
DOI:10.1002/chem.201300827

Reference yield:

: 112-47-0
1,10-Decanediol

: 1446490-23-8
C₂₇H₄₂O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / Inert atmosphere

3.1: titanium(IV) isopropylate; C₂₃H₁₆N₂O₂ / dichloromethane / -40 °C / Inert atmosphere

3.2: 48 h / -40 °C / Inert atmosphere

4.1: dichloromethane / 2.5 h / 0 °C / Inert atmosphere

5.1: methanesulfonic acid; zinc / tetrahydrofuran / Inert atmosphere; Reflux

5.2: Heating

5.3: 2 h / 0 °C / Inert atmosphere

6.1: palladium(II) trifluoroacetate; N-ethyl-N,N-diisopropylamine; bis[2-(diphenylphosphino)phenyl] ether / acetonitrile / 14 h

With titanium(IV) isopropylate; methanesulfonic acid; palladium(II) trifluoroacetate; C₂₃H₁₆N₂O₂; silica gel; sodium hydride; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; bis[2-(diphenylphosphino)phenyl] ether; zinc; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201300827

Reference yield:

: 1446490-16-9
C₁₈H₂₇NO₂

: 1446490-23-8
C₂₇H₄₂O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 2.5 h / 0 °C / Inert atmosphere

2.1: methanesulfonic acid; zinc / tetrahydrofuran / Inert atmosphere; Reflux

2.2: Heating

2.3: 2 h / 0 °C / Inert atmosphere

3.1: palladium(II) trifluoroacetate; N-ethyl-N,N-diisopropylamine; bis[2-(diphenylphosphino)phenyl] ether / acetonitrile / 14 h

With methanesulfonic acid; palladium(II) trifluoroacetate; N-ethyl-N,N-diisopropylamine; bis[2-(diphenylphosphino)phenyl] ether; zinc; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/chem.201300827