C₁₆H₁₈N₂O₃

Base Information

Chemical Name:C₁₆H₁₈N₂O₃
CAS No.:1362624-54-1
Molecular Formula:C₁₆H₁₈N₂O₃
Molecular Weight:286.331
Hs Code.:

C<sub>16</sub>H<sub>18</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₈N₂O₃

Chemical Property:

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Technology Process of C₁₆H₁₈N₂O₃

There total 5 articles about C₁₆H₁₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1362624-59-6
C₂₃H₂₄N₂O₃

: 1362624-54-1
C₁₆H₁₈N₂O₃

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In N,N-dimethyl-formamide; for 24h; under 760.051 Torr;
DOI:10.1021/ml300005w

Reference yield:

: C₁₅H₁₃NO₃

: 1362624-54-1
C₁₆H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0.17 h / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 760.05 Torr

With 5%-palladium/activated carbon; hydrogen; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml300005w

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1362624-54-1
C₁₆H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 0 - 10 °C

2: diphenyl phosphoryl azide; triethylamine / benzene / 5 h / 20 °C / Inert atmosphere; Reflux

3: dichloromethane / 0.17 h / Inert atmosphere

4: 5%-palladium/activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 760.05 Torr

With sodium chlorite; sodium dihydrogenphosphate; diphenyl phosphoryl azide; 5%-palladium/activated carbon; hydrogen; dihydrogen peroxide; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; benzene; 2: Curtius rearrangement;
DOI:10.1021/ml300005w