tetrachloro(1,1-diphenylhydrazido^(2-))(pyridine)tungsten

Base Information

• Chemical Name: tetrachloro(1,1-diphenylhydrazido^(2-))(pyridine)tungsten
• CAS No.: 956100-05-3
• Molecular Formula: C₁₇H₁₅Cl₄N₃W
• Molecular Weight: 586.988
• Mol file: 956100-05-3.mol

Synonyms:

Chemical Property of tetrachloro(1,1-diphenylhydrazido^(2-))(pyridine)tungsten

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tetrachloro(1,1-diphenylhydrazido^(2-))(pyridine)tungsten

There total 1 articles about tetrachloro(1,1-diphenylhydrazido^(2-))(pyridine)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

pyridine (110-86-1) + tungsten(VI) chloride (13283-01-7) + 1,1-Diphenylhydrazine (530-50-7) → tetrachloro(1,1-diphenylhydrazido(2-))(pyridine)tungsten (956100-05-3)

Guidance literature:

In pyridine; under N2; Ph2NNH2 added under stirring to WCl6 in CH2Cl2 at -78°C; stirred for 10 min; solvent removed in vac. during warming to room temp.; pyridine added; stirred for 30 min; solvent removed in vac.; extd. with benzene; extract filtered; solvent removed in vac.; elem. anal.;

DOI:10.1021/ic701151m

upstream raw materials:

pyridine

tungsten(VI) chloride

1,1-Diphenylhydrazine