Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ

Base Information

• Chemical Name: Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ
• CAS No.: 118405-01-9
• Molecular Formula: C₅₀H₆₉N₅O₉
• Molecular Weight: 884.126

Synonyms:

Chemical Property of Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ

There total 6 articles about Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2E,4R,S,5S)-5-<<(1,1-dimethylethoxy)carbonyl>amino>-4-hydroxy-6-phenyl-2-hexenoic acid (99113-32-3,99113-34-5,118386-98-4) → Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ (118405-01-9,124338-98-3,124339-26-0)

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 0.5 h, 2.) room temp.;

DOI:10.1021/jm00164a058

Reference yield:

Methyl (S)-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate (118457-05-9) → Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ (118405-01-9,124338-98-3,124339-26-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

2: 1.1 g / 1 N NaOH / methanol / 2 h / Ambient temperature

3: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With sodium hydroxide; benzotriazol-1-ol; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm00164a058

Reference yield:

[3-((S)-1-tert-Butoxycarbonylamino-2-phenyl-ethyl)-oxiranyl]-acetic acid methyl ester (124266-92-8,124339-16-8) → Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ (118405-01-9,124338-98-3,124339-26-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.1 g / 1 N NaOH / methanol / 2 h / Ambient temperature

2: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00164a058

upstream raw materials:

(2E,4R,S,5S)-5-<<(1,1-dimethylethoxy)carbonyl>amino>-4-hydroxy-6-phenyl-2-hexenoic acid

Methyl (S)-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

[3-((S)-1-tert-Butoxycarbonylamino-2-phenyl-ethyl)-oxiranyl]-acetic acid methyl ester

Boc-L-phenylalaninal

Downstream raw materials:

Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

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