C₁₅H₂₁N₃O₄

Base Information

Chemical Name:C₁₅H₂₁N₃O₄
CAS No.:1366423-08-6
Molecular Formula:C₁₅H₂₁N₃O₄
Molecular Weight:307.349
Hs Code.:

C<sub>15</sub>H<sub>21</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₁N₃O₄

Chemical Property:

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Technology Process of C₁₅H₂₁N₃O₄

There total 6 articles about C₁₅H₂₁N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22323-80-4
(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

: 1366423-08-6
C₁₅H₂₁N₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzene / Reflux

2.1: diisobutylaluminium hydride / hexane; dichloromethane / -78 - 0 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 1.5 h / -40 °C / Inert atmosphere; Molecular sieve

3.2: 89 h / -40 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

5.1: sodium azide; water; ammonium chloride / ethyl methyl ether / 5 h / Reflux

With titanium(IV) isopropylate; sodium azide; L-(+)-diisopropyl tartrate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; ammonium chloride; In tetrahydrofuran; hexane; ethyl methyl ether; dichloromethane; mineral oil; benzene; 1.1: Wittig reaction / 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1021/jo202054g

Reference yield:

: 1366423-06-4
C₈H₁₄O₄

: 1366423-08-6
C₁₅H₂₁N₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

2: sodium azide; water; ammonium chloride / ethyl methyl ether / 5 h / Reflux

With sodium azide; water; tetra-(n-butyl)ammonium iodide; sodium hydride; ammonium chloride; In tetrahydrofuran; ethyl methyl ether; mineral oil;
DOI:10.1021/jo202054g