Technology Process of C15H20O3
There total 6 articles about C15H20O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: iodine; magnesium / tetrahydrofuran / 1.5 h / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / Cooling with ice; Inert atmosphere
3.1: sodium hydroxide / toluene / 60 °C / Inert atmosphere
4.1: tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis(mesityl)imidazolium chloride / tetrahydrofuran; water / 14 h / 66 °C
5.1: hydrogen / dichloromethane / 14 h
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); hydrogen; iodine; magnesium; 1,3-bis(mesityl)imidazolium chloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
4.1: Suzuki coupling;
DOI:10.1002/chem.201102650
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / toluene / 60 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis(mesityl)imidazolium chloride / tetrahydrofuran; water / 14 h / 66 °C
3: hydrogen / dichloromethane / 14 h
With
tris-(dibenzylideneacetone)dipalladium(0); hydrogen; 1,3-bis(mesityl)imidazolium chloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
2: Suzuki coupling;
DOI:10.1002/chem.201102650
