C₃₀H₄₉N₅O₃

Base Information

• Chemical Name: C₃₀H₄₉N₅O₃
• CAS No.: 290354-11-9
• Molecular Formula: C₃₀H₄₉N₅O₃
• Molecular Weight: 527.751
• Mol file: 290354-11-9.mol

Synonyms:

Chemical Property of C₃₀H₄₉N₅O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₉N₅O₃

There total 5 articles about C₃₀H₄₉N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mononitro-p-xylene (89-58-7) → C30H49N5O3 (290354-11-9)

Guidance literature:

Multi-step reaction with 5 steps

1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / 10 h / Heating

2: K₂CO₃ / tetrahydrofuran / 72 h / 20 °C

3: H₂ / PtO₂ / diethyl ether

4: 7.1 g / HCl / diethyl ether

5: pyridine / 12 h / 60 °C

With pyridine; hydrogenchloride; N-Bromosuccinimide; hydrogen; potassium carbonate; dibenzoyl peroxide; platinum(IV) oxide; In tetrahydrofuran; tetrachloromethane; diethyl ether; 1: Bromination / 2: Condensation / 3: Catalytic hydrogenation / 4: Addition / 5: Acylation;

DOI:10.1016/S0968-0896(00)00033-X

Reference yield:

2-nitro-α,α'-dibromo-p-xylene (132733-95-0) → C30H49N5O3 (290354-11-9)

Guidance literature:

Multi-step reaction with 4 steps

1: K₂CO₃ / tetrahydrofuran / 72 h / 20 °C

2: H₂ / PtO₂ / diethyl ether

3: 7.1 g / HCl / diethyl ether

4: pyridine / 12 h / 60 °C

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; 1: Condensation / 2: Catalytic hydrogenation / 3: Addition / 4: Acylation;

DOI:10.1016/S0968-0896(00)00033-X

Reference yield:

C28H45N5O4 (290354-09-5) → C30H49N5O3 (290354-11-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / PtO₂ / diethyl ether

2: 7.1 g / HCl / diethyl ether

3: pyridine / 12 h / 60 °C

With pyridine; hydrogenchloride; hydrogen; platinum(IV) oxide; In diethyl ether; 1: Catalytic hydrogenation / 2: Addition / 3: Acylation;

DOI:10.1016/S0968-0896(00)00033-X

upstream raw materials:

acetic anhydride

mononitro-p-xylene

2-nitro-α,α'-dibromo-p-xylene

C₂₈H₄₇N₅O₂