C₂₀H₂₀ClN₃O₃S*ClH

Base Information

Chemical Name:C₂₀H₂₀ClN₃O₃S*ClH
CAS No.:1277100-10-3
Molecular Formula:C₂₀H₂₀ClN₃O₃S*ClH
Molecular Weight:454.377
Hs Code.:

C<sub>20</sub>H<sub>20</sub>ClN<sub>3</sub>O<sub>3</sub>S*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₀ClN₃O₃S*ClH

Chemical Property:

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Technology Process of C₂₀H₂₀ClN₃O₃S*ClH

There total 6 articles about C₂₀H₂₀ClN₃O₃S*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₈ClN₃O₅S

: 1277100-10-3
C₂₀H₂₀ClN₃O₃S*ClH

Guidance literature:: With hydrogenchloride; In chloroform; at 0 ℃; for 0.5h;
DOI:10.1016/j.ejps.2010.11.010

Reference yield:

: 6310-09-4
2-acetyl-5-chlorothiophene

: 1277100-10-3
C₂₀H₂₀ClN₃O₃S*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: hydroxylamine hydrochloride / ethanol / 6 h / Reflux

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 °C

4.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 24 h / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C

5.2: 4 h / 20 °C

6.1: hydrogenchloride / chloroform / 0.5 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; hydroxylamine hydrochloride; sodium hydride; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010

Reference yield:

: 323594-39-4
3-(bromomethyl)-5-(5-chlorothiophen-2-yl)isoxazole

: 1277100-10-3
C₂₀H₂₀ClN₃O₃S*ClH

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 4 h / 20 °C

2.1: hydrogenchloride / chloroform / 0.5 h / 0 °C

With hydrogenchloride; sodium hydride; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010