MoCl₂(NC₆H₄Cl)2(CH₃OCH₂CH₂OCH₃)

Base Information

• Chemical Name: MoCl₂(NC₆H₄Cl)2(CH₃OCH₂CH₂OCH₃)
• CAS No.: 1361241-55-5
• Molecular Formula: C₁₆H₁₈Cl₄MoN₂O₂
• Molecular Weight: 508.083
• Mol file: 1361241-55-5.mol

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Chemical Property of MoCl₂(NC₆H₄Cl)2(CH₃OCH₂CH₂OCH₃)

Chemical Property:

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Technology Process of MoCl₂(NC₆H₄Cl)2(CH₃OCH₂CH₂OCH₃)

There total 1 articles about MoCl₂(NC₆H₄Cl)2(CH₃OCH₂CH₂OCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

sodium molybdate + 1,2-dimethoxyethane (110-71-4) + o-chloroaniline (95-51-2) → MoCl2(NC6H4Cl)2(CH3OCH2CH2OCH3) (1361241-55-5)

Guidance literature:

With Et₃N; TMSCl; In 1,2-dimethoxyethane; mixt. of amine, Na2MoO4, Et3N and TMSCl in MeOCH2CH2OMe heated at 60°C overnight;

DOI:10.1021/om3000289

Reference yield: 68.0%

2-phenyl-2,2-dimethylethylmagnesium bromide + MoCl2(NC6H4Cl)2(CH3OCH2CH2OCH3) (1361241-55-5) → Mo(NC6H4Cl)2(neophyl)2 (1361241-64-6)

Guidance literature:

In diethyl ether; byproducts: DME; Mo complex reacted with PhCMe2CH2MgBr in Et2O at -35°C;

DOI:10.1021/om3000289

upstream raw materials:

1,2-dimethoxyethane

o-chloroaniline

Downstream raw materials:

Mo(NC₆H₄Cl)2(neophyl)2