1,2-Bis(3-methoxyphenyl)hydrazine

Base Information

• Chemical Name: 1,2-Bis(3-methoxyphenyl)hydrazine
• CAS No.: 1027-32-3
• Molecular Formula: C14H16N2O2
• Molecular Weight: 244.293
• DSSTox Substance ID: DTXSID60590856
• Wikidata: Q82484476
• Mol file: 1027-32-3.mol

Synonyms:1,2-Bis(3-methoxyphenyl)hydrazine;1027-32-3;SCHEMBL8326648;DTXSID60590856

Chemical Property of 1,2-Bis(3-methoxyphenyl)hydrazine

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 244.121177757
• Heavy Atom Count: 18
• Complexity: 214

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC(=C1)NNC2=CC(=CC=C2)OC

Technology Process of 1,2-Bis(3-methoxyphenyl)hydrazine

There total 6 articles about 1,2-Bis(3-methoxyphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(E)-1,2-bis(3-methoxyphenyl)diazene (6319-23-9) → 3,3'-bis(methoxy)diphenyl hydrazine (1027-32-3)

Guidance literature:

With sodium dithionite; In methanol; dichloromethane; water; for 1.5h; Heating;

DOI:10.1055/s-2007-982565

Reference yield: 69.7%

3-nitroanisole (555-03-3) → 3,3'-bis(methoxy)diphenyl hydrazine (1027-32-3)

Guidance literature:

With sodium tetrahydroborate; In dimethyl sulfoxide; at 15 - 50 ℃; for 2h; Solvent; Reagent/catalyst;

Reference yield:

1,2-bis(3-methoxyphenyl)diazene (6319-23-9) → 3,3'-bis(methoxy)diphenyl hydrazine (1027-32-3)

Guidance literature:

With sodium hydroxide; zinc;

DOI:10.1021/ja01100a032

upstream raw materials:

3-nitroanisole

1,2-bis(3-methoxyphenyl)diazene

(E)-1,2-bis(3-methoxyphenyl)diazene

Downstream raw materials:

1,2-bis(3-methoxyphenyl)diazene

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