Technology Process of C58H80N2O10
There total 14 articles about C58H80N2O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: tetra-(n-butyl)ammonium iodide / dimethyl sulfoxide / 110 °C
2: acetyl chloride / 5 - 20 °C
3: hydrazine / ethanol / 80 °C
4: pyridine / 20 °C
5: methanol; sodium methylate / 20 °C
6: sodium hydride / N,N-dimethyl-formamide / 10 - 25 °C
7: hydrogenchloride; water / acetic acid / 75 °C
8: potassium carbonate / dichloromethane / 12 h / 20 °C
9: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran; diethyl ether / -20 °C / Inert atmosphere; Molecular sieve
With
pyridine; hydrogenchloride; methanol; trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; acetyl chloride; hydrazine;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / N,N-dimethyl-formamide / 10 - 25 °C
2: hydrogenchloride; water / acetic acid / 75 °C
3: potassium carbonate / dichloromethane / 12 h / 20 °C
4: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran; diethyl ether / -20 °C / Inert atmosphere; Molecular sieve
With
hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; water; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 20 °C
2: methanol; sodium methylate / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 10 - 25 °C
4: hydrogenchloride; water / acetic acid / 75 °C
5: potassium carbonate / dichloromethane / 12 h / 20 °C
6: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran; diethyl ether / -20 °C / Inert atmosphere; Molecular sieve
With
pyridine; hydrogenchloride; methanol; trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide;