((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂

Base Information

Chemical Name:((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂
CAS No.:1310494-20-2
Molecular Formula:C₅₁H₉₃Ga₃I₂N₆
Molecular Weight:1253.32
Hs Code.:

((CH<sub>3</sub>)3CC(NC<sub>6</sub>H<sub>11</sub>)2)3Ga<sub>3</sub>I<sub>2</sub>

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Chemical Property of ((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂

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Technology Process of ((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂

There total 1 articles about ((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: gallium(I) iodide

: 594-19-4
tert.-butyl lithium

: 538-75-0
dicyclohexyl-carbodiimide

: 1310494-20-2
((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂

Guidance literature:: In toluene; byproducts: gallium; (Ar) to soln. carbodiimide in Et2O at 0°C soln. t-BuLi in hexane was added, stirred overnight, volatiles were removed in vacuo, residue was suspnded in toluene and added at -78°C to GaI in toluene, stirred overnight; volatiles were removed in vacuo, residue was extd. with n-hexane, toluene and THF; elem. anal.;
DOI:10.1039/c1dt10209e

Reference yield:

: 1310494-20-2
((CH₃)3CC(NC₆H₁₁)2)3Ga₃I₂

: 917-54-4
methyllithium

: 75-05-8,26809-02-9
acetonitrile

: 1310494-21-3
((CH₃)3CC(NC₆H₁₁)2)3Ga₃I(NC(CH₃)2)

Guidance literature:: In tetrahydrofuran; toluene; (Ar) soln. MeLi in Et2O was added to acetonitrile, volatiles were removed in vacuo, residue was dissolved in THF, added to soln. Ga complex in toluene at -78°C, stirred overnight; voilatiles were removed in vacuo, residue was extd. with THF;
DOI:10.1039/c1dt10209e