C₂₁H₁₈N₂O₃

Base Information

Chemical Name:C₂₁H₁₈N₂O₃
CAS No.:1382354-41-7
Molecular Formula:C₂₁H₁₈N₂O₃
Molecular Weight:346.386
Hs Code.:

C<sub>21</sub>H<sub>18</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₈N₂O₃

Chemical Property:

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Technology Process of C₂₁H₁₈N₂O₃

There total 4 articles about C₂₁H₁₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1382354-37-1
C₂₂H₂₀N₂O₃

: 1382354-41-7
C₂₁H₁₈N₂O₃

Guidance literature:: C₂₂H₂₀N₂O₃; With lithium hydroxide monohydrate; In tetrahydrofuran; methanol; water; at 20 ℃;

With hydrogenchloride; In water;
DOI:10.1021/jm3002108

Reference yield:

: 33672-82-1
N-(4-nitrophenyl)-N-methylbenzamide

: 1382354-41-7
C₂₁H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; XPhos / tert-butyl alcohol / Reflux

3: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; potassium carbonate; XPhos; In tetrahydrofuran; methanol; ethanol; water; tert-butyl alcohol; 2: Buchwald-Hartwig reaction;
DOI:10.1021/jm3002108

Reference yield:

: 63721-85-7
benzoic acid-(4-amino-N-methyl-anilide)

: 1382354-41-7
C₂₁H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; XPhos / tert-butyl alcohol / Reflux

2: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium hydroxide monohydrate; potassium carbonate; XPhos; In tetrahydrofuran; methanol; water; tert-butyl alcohol; 1: Buchwald-Hartwig reaction;
DOI:10.1021/jm3002108