BICMAP

Base Information

• Chemical Name: BICMAP
• CAS No.: 1157852-82-8
• Molecular Formula: C₄₀H₃₂O₂P₂
• Molecular Weight: 606.64

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Chemical Property of BICMAP

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Technology Process of BICMAP

There total 1 articles about BICMAP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

(+/-)-(2,2',3,3'-tetrahydro-[7,7'-bibenzofuran]-6,6'-diyl)bis(diphenylphosphine oxide) (1156406-05-1) → BICMAP (1157852-82-8,1157852-83-9,1156405-95-6)

Guidance literature:

With trichlorosilane; triethylamine; In m-xylene; at 110 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.02.182

Reference yield: 27.0%

BICMAP (1157852-82-8,1157852-83-9,1156405-95-6) → BICMAP + BICMAP

Guidance literature:

optical yield given as %ee; Resolution of racemate;

DOI:10.1016/j.tetlet.2009.02.182

upstream raw materials:

(+/-)-(2,2',3,3'-tetrahydro-[7,7'-bibenzofuran]-6,6'-diyl)bis(diphenylphosphine oxide)

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