C₂₂H₂₅N₃O₅S

Base Information

Chemical Name:C₂₂H₂₅N₃O₅S
CAS No.:1426329-52-3
Molecular Formula:C₂₂H₂₅N₃O₅S
Molecular Weight:443.524
Hs Code.:

C<sub>22</sub>H<sub>25</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₂H₂₅N₃O₅S

Chemical Property:

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Technology Process of C₂₂H₂₅N₃O₅S

There total 7 articles about C₂₂H₂₅N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426329-51-2
C₂₂H₂₃N₃O₅S

: 1426329-52-3
C₂₂H₂₅N₃O₅S

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; water; at 0 ℃; for 1h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1039/c3ob26994a

Reference yield:

: 171032-74-9
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-glucopyranose

: 1426329-52-3
C₂₂H₂₅N₃O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: boron trifluoride diethyl etherate / chloroform / 0 - 40 °C

2: sodium methylate; water / methanol / 1.5 h

3: toluene-4-sulfonic acid / acetonitrile / 2 h

4: triethylamine; dmap / dichloromethane / 20 °C

5: sodium cyanoborohydride; hydrogenchloride / water; tetrahydrofuran; 1,4-dioxane / 1 h / 0 °C / Molecular sieve; Inert atmosphere

With hydrogenchloride; dmap; boron trifluoride diethyl etherate; water; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetonitrile;
DOI:10.1039/c3ob26994a

Reference yield:

: 90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8
2-deoxy-2-amino glucose

: 1426329-52-3
C₂₂H₂₅N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: triflic azide; potassium carbonate; copper(II) sulfate / water; methanol / 24 h

2: triethylamine; dmap / dichloromethane / 2 h / 20 °C

3: boron trifluoride diethyl etherate / chloroform / 0 - 40 °C

4: sodium methylate; water / methanol / 1.5 h

5: toluene-4-sulfonic acid / acetonitrile / 2 h

6: triethylamine; dmap / dichloromethane / 20 °C

7: sodium cyanoborohydride; hydrogenchloride / water; tetrahydrofuran; 1,4-dioxane / 1 h / 0 °C / Molecular sieve; Inert atmosphere

With hydrogenchloride; dmap; triflic azide; boron trifluoride diethyl etherate; water; sodium methylate; sodium cyanoborohydride; potassium carbonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetonitrile;
DOI:10.1039/c3ob26994a