C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

Base Information

Chemical Name:C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)
CAS No.:1428798-57-5
Molecular Formula:CF₃O₃S*C₂₄H₂₆Cl₂NO₂
Molecular Weight:580.452
Hs Code.:

C<sub>24</sub>H<sub>26</sub>Cl<sub>2</sub>NO<sub>2</sub><sup>(1+)</sup>*CF<sub>3</sub>O<sub>3</sub>S<sup>(1-)</sup>

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Chemical Property of C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

Chemical Property:

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Technology Process of C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

There total 4 articles about C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1428798-29-1
2,6-bis(3-(3-chlorophenoxy)propyl)pyridine

: 333-27-7
methyl trifluoromethanesulfonate

: 1428798-57-5
C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm301564f

Reference yield:

: 33302-52-2
1-chloro-3-(prop-2-yn-1-yloxy)benzene

: 1428798-57-5
C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; triethylamine; trans-bis(triphenylphosphine)palladium dichloride / acetonitrile / Inert atmosphere; Reflux

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C / 1875.19 Torr

3: dichloromethane / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301564f

Reference yield:

: 108-43-0
3-monochlorophenol

: 1428798-57-5
C₂₄H₂₆Cl₂NO₂⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / Reflux

2: copper(l) iodide; triethylamine; trans-bis(triphenylphosphine)palladium dichloride / acetonitrile / Inert atmosphere; Reflux

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C / 1875.19 Torr

4: dichloromethane / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone; acetonitrile; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301564f