1-lithium 2-chloro perfluoro cyclohexene

Base Information

• Chemical Name: 1-lithium 2-chloro perfluoro cyclohexene
• CAS No.: 24512-34-3
• Molecular Formula: C₆ClF₈Li
• Molecular Weight: 266.447
• Mol file: 24512-34-3.mol

Synonyms:

Chemical Property of 1-lithium 2-chloro perfluoro cyclohexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-lithium 2-chloro perfluoro cyclohexene

There total 2 articles about 1-lithium 2-chloro perfluoro cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + 1,2-dichloro-3,3,4,4,5,5,6,6-octafluoro-cyclohexene (336-19-6) → 1-lithium 2-chloro perfluoro cyclohexene (24512-34-3)

Guidance literature:

In diethyl ether;

Reference yield:

→ 1-lithium 2-chloro perfluoro cyclohexene (24512-34-3)

Guidance literature:

1.2-Dichlor-octafluor-cyclohexen-(1), n-Butyl-Li, Et2O, Hexan, -70grad;

DOI:10.1021/jo01257a076

Reference yield: 64.0%

1-lithium 2-chloro perfluoro cyclohexene (24512-34-3) + dichlorodimethylgermanium (1529-48-2) → bis-(2,2'-chloro octafluoro cyclohexenyl-(1,1')) dimethyl germane (50317-04-9)

Guidance literature:

In diethyl ether; reaction at -75°C (15 minutes), heating to 20°C;;

upstream raw materials:

n-butyllithium

1,2-dichloro-3,3,4,4,5,5,6,6-octafluoro-cyclohexene

Downstream raw materials:

bis-(2,2'-chloro octafluoro cyclohexenyl-(1,1')) dimethyl germane

di-(2-chloro octafluoro cyclohexen-⁽¹⁾-yl) mercury