(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

Base Information

Chemical Name:(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid
CAS No.:137407-82-0
Molecular Formula:C₂HF₃O₂*C₃₀H₄₀N₄O₆
Molecular Weight:666.695
Hs Code.:

(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

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Chemical Property of (S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

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Technology Process of (S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

There total 6 articles about (S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117505-35-8,129446-60-2
(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-[(3-Hydroxy-pyridine-2-carbonyl)-amino]-3-{(S)-2-[(4-oxo-piperidine-2-carbonyl)-amino]-2-phenyl-acetoxy}-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid; compound with trifluoro-acetic acid

: 137407-82-0
(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / NaOH (0.5 N) / 2 h / Ambient temperature

2: 99 percent / DCC, DMAP / CH₂Cl₂ / -10 °C

3: 90 percent / DMAP / CH₂Cl₂ / 2 h / Ambient temperature

4: NaOMe / methanol / 24 h / Ambient temperature

5: 74 percent / CH₂Cl₂

With dmap; sodium hydroxide; sodium methylate; dicyclohexyl-carbodiimide; In methanol; dichloromethane;

Reference yield:

: 131286-33-4
(S)-2-{[(S)-1-((R)-2-{(2S,3R)-3-Hydroxy-2-[(3-hydroxy-pyridine-2-carbonyl)-amino]-butyrylamino}-butyryl)-pyrrolidine-2-carbonyl]-methyl-amino}-3-phenyl-propionic acid

: 137407-82-0
(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / DCC, DMAP / CH₂Cl₂ / -10 °C

2: 90 percent / DMAP / CH₂Cl₂ / 2 h / Ambient temperature

3: NaOMe / methanol / 24 h / Ambient temperature

4: 74 percent / CH₂Cl₂

With dmap; sodium methylate; dicyclohexyl-carbodiimide; In methanol; dichloromethane;

Reference yield:

: 137407-78-4
(S)-2-{[(S)-1-((R)-2-{(2S,3R)-3-Hydroxy-2-[(3-hydroxy-pyridine-2-carbonyl)-amino]-butyrylamino}-butyryl)-pyrrolidine-2-carbonyl]-methyl-amino}-3-phenyl-propionic acid benzyl ester

: 137407-82-0
(S)-2-({(S)-1-[(R)-2-((2S,3R)-2-Amino-3-hydroxy-butyrylamino)-butyryl]-pyrrolidine-2-carbonyl}-methyl-amino)-3-phenyl-propionic acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / DMAP / CH₂Cl₂ / 2 h / Ambient temperature

2: NaOMe / methanol / 24 h / Ambient temperature

3: 74 percent / CH₂Cl₂

With dmap; sodium methylate; In methanol; dichloromethane;