1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

Base Information

Chemical Name:1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene
CAS No.:123433-82-9
Molecular Formula:C₂₂H₂₈Si
Molecular Weight:320.55
Hs Code.:

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Chemical Property of 1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

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Technology Process of 1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

There total 5 articles about 1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5-dimethylcyclopent-2-enone: 17197-84-1
5,5-dimethylcyclopent-2-enone

: 123433-82-9
1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / H₂ / 10percent Pd/C / methanol / 6 h / Ambient temperature

2: 84 percent / sodium methoxide / methanol / 16 h / Ambient temperature

3: 92 percent / sodium borohydride, cerium(III) chloride / methanol / 0.08 h / 0 °C

4: 95 percent / Et₃N, N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / Ambient temperature; 2-3 h

5: 1.) copper(I) cyanide, triphenylphosphine / 1.) THF, Et₂O (or Et₂O-pentane), 0 deg C, .) Et₂O (or Et₂O-pentane), 0 deg C, 2-4 h

With dmap; sodium tetrahydroborate; cerium(III) chloride; hydrogen; sodium methylate; copper(l) cyanide; triethylamine; triphenylphosphine; palladium on activated charcoal; In methanol; dichloromethane;

Reference yield:

: 4541-32-6
2,2-dimethylcyclopentanone

: 123433-82-9
1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / sodium methoxide / methanol / 16 h / Ambient temperature

2: 92 percent / sodium borohydride, cerium(III) chloride / methanol / 0.08 h / 0 °C

3: 95 percent / Et₃N, N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / Ambient temperature; 2-3 h

4: 1.) copper(I) cyanide, triphenylphosphine / 1.) THF, Et₂O (or Et₂O-pentane), 0 deg C, .) Et₂O (or Et₂O-pentane), 0 deg C, 2-4 h

With dmap; sodium tetrahydroborate; cerium(III) chloride; sodium methylate; copper(l) cyanide; triethylamine; triphenylphosphine; In methanol; dichloromethane;

Reference yield:

: 146513-84-0
(E)-2-benzylidene-5,5-dimethylcyclopentanol

: 123433-82-9
1-<α-dimethyl(phenyl)silylbenzyl>-3,3-dimethylcyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N, N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / Ambient temperature; 2-3 h

2: 1.) copper(I) cyanide, triphenylphosphine / 1.) THF, Et₂O (or Et₂O-pentane), 0 deg C, .) Et₂O (or Et₂O-pentane), 0 deg C, 2-4 h

With dmap; copper(l) cyanide; triethylamine; triphenylphosphine; In dichloromethane;