(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

Base Information

Chemical Name:(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂
CAS No.:1365064-34-1
Molecular Formula:C₃₅H₄₈Cl₂FeN₄
Molecular Weight:651.546
Hs Code.:

(2,6-(2,6-(i)Pr<sub>2</sub>-C<sub>6</sub>H<sub>3</sub>N=CMe)2-4-Me<sub>2</sub>N-C<sub>5</sub>H<sub>2</sub>N)FeCl<sub>2</sub>

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Chemical Property of (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

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Technology Process of (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

There total 1 articles about (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1365064-31-8
2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N

: iron(II) chloride

: 1365064-34-1
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

Guidance literature:: In tetrahydrofuran; under N2; by a react. of FeCl2 (0.65 mmol) and a ligand (0.68 mmol) in THF; stirring for 12 h; addn. of pentane; filtering and washing with Et2O; elem. anal.;
DOI:10.1021/om201212m

Reference yield: 65.0%

: 201230-82-2
carbon monoxide

: 1365064-34-1
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

: 1365064-37-4
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(CO)2

Guidance literature:: With Na; Hg; In toluene; under N2; by a react. of Fe-contg. compd. (0.38 mmol) in toluene with CO(1 atm) in the presence of sodium amalgam (prepd. from Hg and Na in tol uene); stirring for 24 h; the mixt. was decanted away from the amalgam and filtered through a pad of Celite; the solvent was removed in vac.; recrystn. from pentane/etherat -35°C; elem. anal.;
DOI:10.1021/om201212m

Reference yield: 39.0%

: 1365064-34-1
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

: 7727-37-9
nitrogen

: 1365064-41-0
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2

Guidance literature:: With Na; Hg; In tetrahydrofuran; toluene; under N2; by a react. of Fe-contg. compd. (0.77 mmol) in toluene and THFwith N2 (1 atm) in the presence of sodium amalgam (prepd. from Hg and N a in toluene); stirring for 3 h; the mixt. was decanted away from the amalgam and concd. in vac. to remove THF; the residue was extd. with pentane, filtered through a pad of Celite and concd.; the soln. was stored at -35°C and deposited as solid;
DOI:10.1021/om201212m