2-phenyl-4-formyl-5-methylmercaptothiazole

Base Information

Chemical Name:2-phenyl-4-formyl-5-methylmercaptothiazole
CAS No.:73725-38-9
Molecular Formula:C₁₁H₉NOS₂
Molecular Weight:235.331
Hs Code.:

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Chemical Property of 2-phenyl-4-formyl-5-methylmercaptothiazole

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Technology Process of 2-phenyl-4-formyl-5-methylmercaptothiazole

There total 5 articles about 2-phenyl-4-formyl-5-methylmercaptothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 73725-37-8
2-phenyl-4-formyl-5-mercaptothiazole

: 74-88-4
methyl iodide

: 73725-38-9
2-phenyl-4-formyl-5-methylmercaptothiazole

Guidance literature:: With sodium methylate; In methanol; for 2h; Heating;
DOI:10.1007/BF00475385

Reference yield:

: 6330-48-9
thiohippuric acid

: 73725-38-9
2-phenyl-4-formyl-5-methylmercaptothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) phosphorus trichloride, 2.) phosphorus oxychloride / 1.) diethyl ether, 20 deg C, 30 min, 2.) 100 deg C, 7 h.

2: 90 percent / potassium hydrosulfide / H₂O; methanol / 2 h / Heating

3: 64 percent / sodium methoxide / methanol / 2 h / Heating

With sodium methylate; potassium hydrosulfide; trichlorophosphate; phosphorus trichloride; In methanol; water;
DOI:10.1007/BF00475385

Reference yield:

: 4264-48-6
2-phenyl-4-formyl-5-chlorothiazole

: 73725-38-9
2-phenyl-4-formyl-5-methylmercaptothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / potassium hydrosulfide / H₂O; methanol / 2 h / Heating

2: 64 percent / sodium methoxide / methanol / 2 h / Heating

With sodium methylate; potassium hydrosulfide; In methanol; water;
DOI:10.1007/BF00475385