Technology Process of C45H56N4O9
There total 3 articles about C45H56N4O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
1.2: Saturated solution
2.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / solid phase reaction
2.2: 4 h / solid phase reaction
2.3: solid phase reaction
With
lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/psc.1256
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2.2: Saturated solution
3.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / solid phase reaction
3.2: 4 h / solid phase reaction
3.3: solid phase reaction
With
lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/psc.1256
- Guidance literature:
-
C13H18NO3Pol; 3-(allyloxycarbonylamino)propanal;
With
sodium cyanoborohydride; acetic acid;
In
N,N-dimethyl-formamide;
solid phase reaction;
Fmoc-Asn(Dmcp)-OH;
With
1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU;
for 4h;
solid phase reaction;
With
trifluoroacetic acid;
In
dichloromethane;
solid phase reaction;
DOI:10.1002/psc.1256
