1--2,2,3-tris(carbomethoxy)cyclobutane methiodide

Base Information

• Chemical Name: 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide
• CAS No.: 72541-98-1
• Molecular Formula: C₁₉H₂₆NO₆*I
• Molecular Weight: 491.323
• Mol file: 72541-98-1.mol

Synonyms:

Chemical Property of 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide

There total 5 articles about 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1--2,2,3-tris(carbomethoxy)cyclobutane (72541-97-0) + methyl iodide (74-88-4) → 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide (72541-98-1)

Guidance literature:

for 1h;

DOI:10.1021/jo01293a015

Reference yield:

4-dimethylamino-benzaldehyde (100-10-7) → 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide (72541-98-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1) Mg / 1) diethyl ether, 1h; 2) diethyl ether, 3h

2: flash distillation at 150 deg C under vacuum

3: 30 percent / acetonitrile / Heating

4: 100 percent / 1 h

With magnesium; In acetonitrile;

DOI:10.1021/jo01293a015

Reference yield:

ethene-1,1,2-tricarboxylic acid trimethyl ester (51175-48-5) → 1--2,2,3-tris(carbomethoxy)cyclobutane methiodide (72541-98-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 30 percent / acetonitrile / Heating

2: 100 percent / 1 h

In acetonitrile;

DOI:10.1021/jo01293a015

upstream raw materials:

1--2,2,3-tris(carbomethoxy)cyclobutane

methyl iodide

ethene-1,1,2-tricarboxylic acid trimethyl ester

1-[4-(N,N-dimethylamino)phenyl]ethanol