(((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane

Base Information

Chemical Name:(((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane
CAS No.:765277-93-8
Molecular Formula:C₇₂H₁₄₀Fe₄N₄O₁₂P₄Si₈
Molecular Weight:1825.89
Hs Code.:

(((PMe<sub>3</sub>Fe)(O<sub>3</sub>Si(2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>)N(SiMe<sub>3</sub>)))4 ferric siloxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane

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Technology Process of (((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane

There total 1 articles about (((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 22999-67-3,133009-01-5
tris[bis(trimethylsilyl)amido]iron(III)

: 163631-37-6
(2,6-iPr2C6H3)N(SiMe3)Si(OH)3

: 594-09-2
trimethylphosphane

: 765277-93-8
(((PMe₃Fe)(O₃Si(2,6-iPr₂C₆H₃)N(SiMe₃)))4 ferric siloxane

Guidance literature:: In hexane; at room temp.; Fe-complex in hexane slowly added to suspn. of silanetriol in the same solvent; mixt. stirred for 72 h; green soln. turned to greenish brown; solvent, hexamethyldisilazane removed in vacuo; recrystn. from THF/toluene=0.05/1 with PMe3 at room temp. for 2 wk; toluene removed by drying under vac.; detd. by IR, ESIMS, elem. anal.;
DOI:10.1002/anie.200453740