(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

Base Information

Chemical Name:(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene
CAS No.:101210-40-6
Molecular Formula:C₃₈H₄₅N₃O₁₄
Molecular Weight:767.787
Hs Code.:

(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

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Chemical Property of (E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

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Technology Process of (E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

There total 4 articles about (E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101210-39-3
Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

: 101210-38-2
t-Butyl 5-formyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrole-2-carboxylate

: 101210-40-6,101210-41-7
(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

: 101210-41-7
(Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

Guidance literature:: With methylamine hydrochloride; potassium acetate; In methanol; at 50 ℃; for 7.3h; Yield given. Yields of byproduct given;

Reference yield:

: 57529-24-5
benzyl 5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrole-2-carboxylate

: 101210-40-6,101210-41-7
(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / potassium acetate, methylamine hydrochloride / methanol / 2 h / 50 °C

2: 87 percent / NaBH₄ / CH₂Cl₂; methanol / 0.03 h

3: potassium acetate, methylamine hydrochloride / methanol / 7.3 h / 50 °C

With sodium tetrahydroborate; methylamine hydrochloride; potassium acetate; In methanol; dichloromethane;

Reference yield:

: 116683-95-5
(E)-Benzyl 4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethenyl)pyrrole-2-carboxylate

: 101210-40-6,101210-41-7
(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaBH₄ / CH₂Cl₂; methanol / 0.03 h

2: potassium acetate, methylamine hydrochloride / methanol / 7.3 h / 50 °C

With sodium tetrahydroborate; methylamine hydrochloride; potassium acetate; In methanol; dichloromethane;