3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide

Base Information

Chemical Name:3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide
CAS No.:35423-52-0
Molecular Formula:C₁₈H₂₈N₂O₆S
Molecular Weight:400.496
Hs Code.:
Mol file:35423-52-0.mol

Synonyms:3-(3’-diethylaminopropyl-(1’)-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide

Suppliers and Price of 3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide

Chemical Property:

Vapor Pressure:2.13E-14mmHg at 25°C
Boiling Point:600.9°Cat760mmHg
Flash Point:317.2°C
PSA：106.04000
Density:1.22g/cm³
LogP:3.10300

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide

There total 4 articles about 3-(3'-diethylaminopropyl-(1')-carbamoyl)-6,7-dimethoxy-1-thiaisochroman-1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39906-73-5
3-Chlorcarbonyl-6,7-dimethoxy-1-thiaisochroman-1,1-dioxid

: 104-78-9
diethylaminopropylamine

: 35423-52-0
6,7-Dimethoxy-1,1-dioxo-3,4-dihydro-1H-1λ⁶-benzo[c][1,2]oxathiine-3-carboxylic acid (3-diethylamino-propyl)-amide

Guidance literature:: With sodium hydroxide; In toluene; at 5 - 10 ℃; for 1h;

Reference yield:

: 14612-07-8
α-Chlor-β-(3,4-dimethoxyphenyl)propionsaeurenitril

: 35423-52-0
6,7-Dimethoxy-1,1-dioxo-3,4-dihydro-1H-1λ⁶-benzo[c][1,2]oxathiine-3-carboxylic acid (3-diethylamino-propyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 72.4 percent / conc. H₂SO₄ / H₂O / 1) 24 h, RT, 2) 48 h, 90 deg C

2: SOCl₂ / 8 h / Heating

3: NaOH / toluene / 1 h / 5 - 10 °C

With sodium hydroxide; thionyl chloride; sulfuric acid; In water; toluene;

Reference yield:

: 29281-16-1
3,4-dihydro-6,7-dimethoxy,2,1-benzoxathiin-3-carboxylic acid

: 35423-52-0
6,7-Dimethoxy-1,1-dioxo-3,4-dihydro-1H-1λ⁶-benzo[c][1,2]oxathiine-3-carboxylic acid (3-diethylamino-propyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 8 h / Heating

2: NaOH / toluene / 1 h / 5 - 10 °C

With sodium hydroxide; thionyl chloride; In toluene;