Technology Process of C27H26N2O4S
There total 9 articles about C27H26N2O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / toluene
2: N-ethyl-N,N-diisopropylamine / acetonitrile
With
thionyl chloride; N-ethyl-N,N-diisopropylamine;
In
toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 9 steps
1: sodium tetrahydroborate / methanol
2: 1H-imidazole
3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)
4: n-butyllithium
5: hydroxylamine hydrochloride; triethylamine / methanol; dichloromethane
6: pyridine; N-chloro-succinimide / chloroform
7: tetrabutyl ammonium fluoride / tetrahydrofuran
8: thionyl chloride / toluene
9: N-ethyl-N,N-diisopropylamine / acetonitrile
With
pyridine; 1H-imidazole; sodium tetrahydroborate; N-chloro-succinimide; n-butyllithium; thionyl chloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine; N-chloro-succinimide / chloroform
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: thionyl chloride / toluene
4: N-ethyl-N,N-diisopropylamine / acetonitrile
With
pyridine; N-chloro-succinimide; thionyl chloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
