Technology Process of C18H31FN2
There total 4 articles about C18H31FN2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen;
In
methanol;
for 24h;
under 760.051 Torr;
Inert atmosphere;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium fluoride; 18-crown-6 ether / tetrahydrofuran / 36 h / Reflux; Inert atmosphere
2: 5%-palladium/activated carbon; hydrogen / methanol / 24 h / 760.05 Torr / Inert atmosphere
With
potassium fluoride; 18-crown-6 ether; 5%-palladium/activated carbon; hydrogen;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate; pyridine / 2 h / Inert atmosphere; Reflux
2: potassium fluoride; 18-crown-6 ether / tetrahydrofuran / 36 h / Reflux; Inert atmosphere
3: 5%-palladium/activated carbon; hydrogen / methanol / 24 h / 760.05 Torr / Inert atmosphere
With
pyridine; potassium fluoride; 18-crown-6 ether; 5%-palladium/activated carbon; hydrogen; trichlorophosphate;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201304161