phenylantimony(III) bis(6-chloro-5-methoxyisatin)

Base Information

• Chemical Name: phenylantimony(III) bis(6-chloro-5-methoxyisatin)
• CAS No.: 152582-19-9
• Molecular Formula: C₂₄H₁₅Cl₂N₂O₆Sb
• Molecular Weight: 620.049
• Mol file: 152582-19-9.mol

Synonyms:

Chemical Property of phenylantimony(III) bis(6-chloro-5-methoxyisatin)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of phenylantimony(III) bis(6-chloro-5-methoxyisatin)

There total 1 articles about phenylantimony(III) bis(6-chloro-5-methoxyisatin) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

6-chloro-5-methoxy-isatin (85778-01-4) + dichlorophenylstibine (5035-52-9) → phenylantimony(III) bis(6-chloro-5-methoxyisatin) (152582-19-9)

Guidance literature:

With triethylamine; In methanol; byproducts: NHEt3Cl; stirring of a soln. of Sb-compd. in anhyd. methanol and isatin-compd. in methanol in presence of triethylamine at room temp. (30°C) for 4 h under an anhyd. and O2 free N2 atmosphere; filtn. under N2, removal of NEt3HCl, concn. of filtrate in vacuo, recrystn. from petroleum ether, elem. anal.;

upstream raw materials:

6-chloro-5-methoxy-isatin

dichlorophenylstibine