Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

Base Information

Chemical Name:Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester
CAS No.:112260-54-5
Molecular Formula:C₂₃H₂₂Cl₃F₃O₈S
Molecular Weight:621.843
Hs Code.:

Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

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Chemical Property of Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

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Technology Process of Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

There total 2 articles about Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 112260-54-5
Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 13 percent / tetra-n-butylammonium bromide, sodium hydroxide / H₂O / 13 h / Ambient temperature

2: pyridine / CH₂Cl₂

With pyridine; sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water;
DOI:10.1139/v87-070

Reference yield:

: 109363-12-4
2,2,2-trichloroethyl 4,6-O-benzylidene-β-D-glucopyranoside

: 112260-54-5
Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 13 percent / tetra-n-butylammonium bromide, sodium hydroxide / H₂O / 13 h / Ambient temperature

2: pyridine / CH₂Cl₂

With pyridine; sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water;
DOI:10.1139/v87-070

Reference yield:

: 112260-54-5
Trifluoro-methanesulfonic acid (4aR,6R,7R,8S,8aR)-8-benzyloxy-2-phenyl-6-(2,2,2-trichloro-ethoxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

: 112260-55-6
2,2,2-trichloroethyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-fluoro-β-D-mannopyranoside

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In dichloromethane; for 5h; Yield given; Heating;
DOI:10.1139/v87-070