(2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride

Base Information

• Chemical Name: (2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride
• CAS No.: 1198151-85-7
• Molecular Formula: C₃₀H₂₃ClOP₂PdS₂
• Molecular Weight: 667.465
• Mol file: 1198151-85-7.mol

Synonyms:

Chemical Property of (2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride

There total 1 articles about (2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + diphenylthiophosphonic acid O-(3-diphenylthiophosphoryl)phenyl ester (1198151-81-3) → (2-[(diphenylthiophosphoryl)oxy]-6-(diphenylthiophosphoryl)phenyl)-palladium chloride (1198151-85-7)

Guidance literature:

In methanol; dichloromethane; (inert atm.); soln. of palladium complex in CH2Cl2 was added to soln. ofester in CH2Cl2, in 1 h reaction mixt was poured into MeOH, left under ambient conditions for 4 d; filtered, evapd., washed with ether, filtered, crystd. from CH2Cl2-Et2O (1:2), elem. anal.;

DOI:10.1039/b907644a

upstream raw materials:

bis(benzonitrile)palladium(II) dichloride

diphenylthiophosphonic acid O-(3-diphenylthiophosphoryl)phenyl ester