Technology Process of diphenylthiophosphonic acid O-(3-diphenylthiophosphoryl)phenyl ester
There total 5 articles about diphenylthiophosphonic acid O-(3-diphenylthiophosphoryl)phenyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
m-hydroxyphenyl(diphenyl)phosphine sulfide;
With
N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide;
In
water; benzene;
diphenylthiophosphinoyl chloride;
In
water; benzene;
at 20 - 60 ℃;
for 2.5h;
DOI:10.1039/b907644a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / tetrahydrofuran / 0 - 5 °C / Inert atmosphere
1.2: 2 h / 50 - 55 °C / Inert atmosphere
2.1: sulfur / benzene / 72 h
3.1: pyridine hydrochloride / 5 h / 180 - 190 °C
4.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; benzene
4.2: 2.5 h / 20 - 60 °C
With
N-benzyl-N,N,N-triethylammonium chloride; pyridine hydrochloride; sulfur; magnesium; sodium hydroxide;
In
tetrahydrofuran; water; benzene;
DOI:10.1039/b907644a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / tetrahydrofuran / 0 - 5 °C / Inert atmosphere
1.2: 2 h / 50 - 55 °C / Inert atmosphere
2.1: sulfur / benzene / 72 h
3.1: pyridine hydrochloride / 5 h / 180 - 190 °C
4.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; benzene
4.2: 2.5 h / 20 - 60 °C
With
N-benzyl-N,N,N-triethylammonium chloride; pyridine hydrochloride; sulfur; magnesium; sodium hydroxide;
In
tetrahydrofuran; water; benzene;
DOI:10.1039/b907644a
