2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid

Base Information

• Chemical Name: 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid
• CAS No.: 55380-70-6
• Molecular Formula: 2C₇H₈O₃S*C₂₆H₄₁N₅O₄S
• Molecular Weight: 864.118
• Mol file: 55380-70-6.mol

Synonyms:

Chemical Property of 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid

There total 3 articles about 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(dimethylamino)naphth-1-ylsulfonyl chloride (605-65-2) → 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid (55380-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / H₂O; diethyl ether / 48 h / Ambient temperature

2: benzene / 3 h / Heating

With potassium carbonate; In diethyl ether; water; benzene;

DOI:10.1021/jm00182a003

Reference yield:

L-arginine (74-79-3,157-06-2,7004-12-8,7200-25-1,25212-18-4) → 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid (55380-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / H₂O; diethyl ether / 48 h / Ambient temperature

2: benzene / 3 h / Heating

With potassium carbonate; In diethyl ether; water; benzene;

DOI:10.1021/jm00182a003

Reference yield:

2-Ethylhexyl alcohol (104-76-7) + toluene-4-sulfonic acid (104-15-4) + Nα-dansyl-L-arginine (4307-78-2,28217-22-3,71869-46-0) → 2-(5-Dimethylamino-naphthalene-1-sulfonylamino)-5-guanidino-pentanoic acid 2-ethyl-hexyl ester; compound with toluene-4-sulfonic acid (55380-70-6)

Guidance literature:

In benzene; for 3h; Heating;

DOI:10.1021/jm00182a003

upstream raw materials:

2-Ethylhexyl alcohol

toluene-4-sulfonic acid

N^α-dansyl-L-arginine

5-(dimethylamino)naphth-1-ylsulfonyl chloride