C₄₄H₇₀N₈

Base Information

• Chemical Name: C₄₄H₇₀N₈
• CAS No.: 1209481-32-2
• Molecular Formula: C₄₄H₇₀N₈
• Molecular Weight: 711.093
• Mol file: 1209481-32-2.mol

Synonyms:

Chemical Property of C₄₄H₇₀N₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₇₀N₈

There total 8 articles about C₄₄H₇₀N₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C44H68N8 → C44H70N8 (1209481-32-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201002871

Reference yield:

1,3,5-tris{[(trans-2'-aminocyclohexyl)amino]methyl}-2,4,6-triethylbenzene (1209481-43-5) → C44H70N8 (1209481-32-2)

Guidance literature:

Multi-step reaction with 4 steps

1: chloroform / 12 h / 70 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

3: chloroform / 12 h / 20 °C / Inert atmosphere

4: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol; chloroform;

DOI:10.1002/chem.201002871

Reference yield:

1,3,5-tris[methyl-(tert-butoxycarbonyl-trans-1,2-diaminocyclohexyl)]-2,4,6-triethylbenzene (1209481-28-6) → C44H70N8 (1209481-32-2)

Guidance literature:

Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: chloroform / 12 h / 70 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

4: chloroform / 12 h / 20 °C / Inert atmosphere

5: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; trifluoroacetic acid; In methanol; dichloromethane; chloroform;

DOI:10.1002/chem.201002871

upstream raw materials:

1,3,5-tris{[(trans-2'-aminocyclohexyl)amino]methyl}-2,4,6-triethylbenzene

CN₁₉_17

1,3,5-tris[methyl-(tert-butoxycarbonyl-trans-1,2-diaminocyclohexyl)]-2,4,6-triethylbenzene

1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene